Table of Peaks
No. 	(ppm) 	(Hz) 	Height
1 	0.66 	327.4 	0.9739 	
2 	0.81 	404.7 	1.0000 	
3 	0.86 	430.2 	0.7674 	
4 	0.87 	432.5 	0.8409 	
5 	0.87 	436.8 	0.8522 	
6 	0.88 	439.0 	0.8681 	
7 	0.90 	449.2 	0.5704 	
8 	0.91 	455.7 	0.5965 	
9 	0.94 	469.8 	0.1179 	
10 	0.95 	473.9 	0.1299 	
11 	0.97 	484.1 	0.1670 	
12 	0.97 	487.0 	0.1989 	
13 	0.99 	493.6 	0.1576 	
14 	1.00 	497.3 	0.2130 	
15 	1.00 	500.6 	0.1695 	
16 	1.02 	507.9 	0.1445 	
17 	1.02 	511.4 	0.1322 	
18 	1.04 	517.4 	0.1133 	
19 	1.05 	523.6 	0.1133 	
20 	1.06 	529.9 	0.1054 	
21 	1.07 	533.5 	0.1520 	
22 	1.09 	543.0 	0.2246 	
23 	1.11 	553.3 	0.2374 	
24 	1.12 	557.9 	0.2696 	
25 	1.12 	562.2 	0.2111 	
26 	1.13 	566.0 	0.2277 	
27 	1.14 	570.7 	0.2059 	
28 	1.25 	623.5 	0.1480 	
29 	1.25 	627.2 	0.1739 	
30 	1.26 	631.0 	0.2523 	
31 	1.27 	634.5 	0.2860 	
32 	1.28 	639.3 	0.2806 	
33 	1.29 	643.7 	0.1842 	
34 	1.29 	647.1 	0.1828 	
35 	1.30 	651.4 	0.2372 	
36 	1.33 	663.3 	0.2876 	
37 	1.34 	672.2 	0.2303 	
38 	1.35 	673.9 	0.2303 	
39 	1.36 	677.3 	0.2128 	
40 	1.37 	685.3 	0.2109 	
41 	1.39 	693.9 	0.1382 	
42 	1.47 	735.7 	0.0852 	
43 	1.48 	739.0 	0.0914 	
44 	1.50 	749.0 	0.0986 	
45 	1.51 	753.6 	0.1330 	
46 	1.52 	760.3 	0.1158 	
47 	1.53 	766.8 	0.1246 	
48 	1.55 	773.8 	0.2451 	
49 	1.58 	788.9 	0.6668 	
50 	1.64 	819.4 	0.0487 	
51 	1.65 	822.7 	0.0801 	
52 	1.65 	826.2 	0.0823 	
53 	1.66 	829.7 	0.0540 	
54 	1.66 	832.1 	0.0537 	
55 	1.67 	835.7 	0.0768 	
56 	1.68 	839.0 	0.0761 	
57 	1.69 	842.4 	0.0492 	
58 	1.69 	846.9 	0.0633 	
59 	1.70 	850.4 	0.0906 	
60 	1.71 	853.9 	0.0684 	
61 	1.72 	860.2 	0.0606 	
62 	1.73 	863.6 	0.0841 	
63 	1.73 	867.2 	0.0600 	
64 	1.78 	887.6 	0.0455 	
65 	1.79 	893.6 	0.0851 	
66 	1.79 	896.8 	0.1022 	
67 	1.80 	900.7 	0.0901 	
68 	1.81 	902.8 	0.1011 	
69 	1.81 	906.5 	0.1113 	
70 	1.82 	909.8 	0.1026 	
71 	1.83 	915.7 	0.0738 	
72 	1.84 	919.5 	0.0473 	
73 	1.85 	925.2 	0.0372 	
74 	1.95 	974.8 	0.0452 	
75 	1.96 	978.2 	0.0762 	
76 	1.96 	981.4 	0.0560 	
77 	1.98 	987.4 	0.0562 	
78 	1.98 	990.7 	0.0765 	
79 	1.99 	994.0 	0.0522 	
80 	3.59 	1794.6 	0.0472 	

Table of Multiplets
No. 	Shift1 (ppm) 	Hs 	Type 	J (Hz) 	Atom1 	Multiplet1 	 (ppm)
1 	0.66 	2 	s 	- 	20 	M03 	0.63 .. 0.68
2 	0.81 	2 	s 	- 	19 	M02 	0.79 .. 0.83
3 	0.87 	5 	dd 	6.60 2.21 	26 28 	M04 	0.85 .. 0.89
4 	0.91 	3 	d 	6.52 	27 	M05 	0.89 .. 0.92
5 	1.04 	10 	m 	- 	5a 7a 22 11 9 24 13 17 23 	M12 	0.94 .. 1.18
6 	1.31 	9 	m 	- 	14 6 23 21 22 2 	M11 	1.23 .. 1.40
7 	1.52 	5 	m 	- 	16 25 11 12 	M10 	1.46 .. 1.61
8 	1.66 	1 	qd 	6.81 6.41 3.34 	15 	M08 	1.63 .. 1.69
9 	1.71 	1 	td 	13.24 3.50 	3 	M07 	1.69 .. 1.74
10 	1.81 	2 	m 	- 	2 10 	M09 	1.77 .. 1.86
11 	1.97 	1 	td 	12.56 3.28 	17 	M06 	1.95 .. 2.00
12 	3.60 	1 	s 	- 	1 	M01 	3.55 .. 3.66

Table of Assignments
No. 	Atom 	Exp. Shift (ppm) 	Multiplet
1 	20 	0.66 	M03
2 	19 	0.81 	M02
3 	26 	0.87 	M04
4 	28 	0.87 	M04
5 	27 	0.91 	M05
6 	5a 	1.04 	M12
7 	7a 	1.04 	M12
8 	22 	1.04 	M12
9 	11 	1.04 	M12
10 	9 	1.04 	M12
11 	24 	1.04 	M12
12 	13 	1.04 	M12
13 	17 	1.04 	M12
14 	23 	1.04 	M12
15 	14 	1.31 	M11
16 	6 	1.31 	M11
17 	23 	1.31 	M11
18 	21 	1.31 	M11
19 	22 	1.31 	M11
20 	2 	1.31 	M11
21 	16 	1.52 	M10
22 	25 	1.52 	M10
23 	11 	1.52 	M10
24 	12 	1.52 	M10
25 	15 	1.66 	M08
26 	3 	1.71 	M07
27 	2 	1.81 	M09
28 	10 	1.81 	M09
29 	17 	1.97 	M06
30 	1 	3.60 	M01
